Reference of 1122-62-9, In the chemical reaction process,reaction time,type of solvent,can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product.An updated downstream synthesis route of 1122-62-9 as follows.
General procedure: A mixture of ketone (1 mmol), a known mole percent of the catalystand KOH (0.06 mmol) was dissolved in 2-propanol (5 mL), and the mixture was heated under reflux for the desired period oftime. The catalyst was removed as precipitate from the reactionmixture by the addition of diethyl ether followed by filtrationand subsequent neutralization with 5 mL of 1 M HCl. Then theether layer was passed through a short path of silica gel and the filtratewas subjected to GC analysis for identification andquantification.
These compound has a wide range of applications. It is believed that with the continuous development of the source of the synthetic route,1122-62-9, its application will become more common.
Reference:
Article; Chowdhury, Nabanita Saha; Guharoy, Chhandasi; Butcher, Ray J.; Bhattacharya, Samaresh; Inorganica Chimica Acta; vol. 406; (2013); p. 20 – 26;,
Pyridine – Wikipedia,
Pyridine | C5H5N – PubChem