Synthetic Route of 114-33-0, As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 114-33-0, name is N-Methylnicotinamide, molecular formula is C7H8N2O, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below.
Appropriate nitrogen donor ligand (1 mmol) was added to an aqueous solution of copper(II) acetate (0.5 mmol) under stirring. After a few minutes, x-methylsalicylic acid (1 mmol) and the necessary amount of solvent (ethanol or acetonitrile) were added to reach the final volume (30-40 mL). Eventually, the reaction mixture was stirred for few days at room temperature until the reaction finished. The precipitate was filtered off and the mother liquids were left to crystallize at room temperature and the crystals were dried at room temperature. The obtained crystals were suitable for X-ray structure determination.
While traditionally a conservative industry, chemical producers will need to modernize their PR strategies to stay relevant.we look forward to future research findings about 114-33-0, N-Methylnicotinamide.
Reference:
Article; Pucho?ova, Miroslava; ?vorec, Jozef; ?vorc, Lubomir; Valigura, Du?an; Chemical Papers; vol. 70; 1; (2016); p. 75 – 81;,
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