Recommanded Product: 91-02-1. Recently I am researching about SELECTIVE REDUCTIVE AMINATION; DENITROGENATIVE TRANSANNULATION; N-TOSYLHYDRAZONES; AMINES SYNTHESIS; HYDRAZONES; REAGENTS, Saw an article supported by the CNRSCentre National de la Recherche Scientifique (CNRS)European Commission; Univ. Paris-Sud; La Ligue Contre le Cancer through an Equipe Labellisee 2014 grant; ANRFrench National Research Agency (ANR) [ANR-10-LABX-33]. Published in WILEY-V C H VERLAG GMBH in WEINHEIM ,Authors: Lamaa, D; Lin, HP; Bzeih, T; Retailleau, P; Alami, M; Hamze, A. The CAS is 91-02-1. Through research, I have a further understanding and discovery of Phenyl(pyridin-2-yl)methanone
A new metal-free procedure allowing Csp(3)-N bond formation through coupling of pyridotriazoles and weakly nucleophilic anilines has been developed. This sustainable reaction shows high tolerance towards functional groups (ketones, free alcohols) leading to 2-picolylamine derivatives. The key to our success is the use of a catalytic amount of TBAB and water as a co-solvent leading to the formation of pyridylalkylamine derivatives. As this coupling tolerates the presence of Csp(2)-Br bond on both partners of the reaction, we performed a sequential one-pot reaction between functionalized triazolopyridines and anilines followed by a second coupling with N-tosylhydrazones leading to the formation of Csp(3)-N and Csp(2)-Csp(2) bonds.
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Reference:
Pyridine – Wikipedia,
,Pyridine | C5H5N – PubChem